Poison Ivy/Riddler team up of course.
Hush
The Phantasm (the Andrea Beaumont version)
. . . Scarface.
However, if we could've picked a villain from one of the previous films, then I would choose Mr. Freeze. Heart of Ice was one of the best Batman: TAS episodes and I really appreciate the re-writing of Freeze's character. I know Batman and Robin incorporated some elements of it but I'd like to see a more serious take.
I'd like to see Clayface, but Clayface as originally intended, not the 90s cartoon sci-fi version.
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